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KMID : 0614019890050010015
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Journal of Pharmaceutical Sciences (C.N.U.)
1989 Volume.5 No. 1 p.15 ~ p.21
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A Study on the Optimum Manufacturing Conditions of Synthetic Aluminum Silicate
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Lee Gye-Ju
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Abstract
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The optimum reaction conditions for the acid consuming capacity of aluminum silicate synthesized from the reaction of sodium silicate solution and potassium aluminum sulfate solution were investigated by Box-Wilson experimental design, and the micromeritic properties were examined by the means of BET N_2 adsorption, Hg penetrometer and methylen blue adsorption. The chemical composition of the samples were analyzed by gravitic method. The results were found to be as follows: optimum reaction temperature 54.7 ℃, both concentrations of reactant soln 15.7%, reactants molar ratio (Al/Si) 0.5 and drying temperature 65.0 ℃.
The acid consuming capacity of the sample prepared by above optimum conditions was 68 ㎖ and the chemical composition was Al_2O_3·3.6SiO_2·3H_2O. The relationship between acid consuming capacity and micromertic properties could not found in the range of experiments. Therefore, it is assumed that the acid consuming mechanism of aluminum silicate depends on the neutralization of Al_2O_3 and buffer action of SiO_2 in sample.
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KEYWORD
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Acid consuming capacity, Box-Wilson experimental design, micromeritic properties, BET N_2 adsorption, Hg penetrometer
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